Publications and communications in the field of "Amount of substance and chemistry" by authors of the French metrology network in 2011

Publications

ALASONATI E. et SLAVEYKOVA V.I., “Composition and molar mass characterisation of bacterial extracellular polymeric substances by using chemical, spectroscopic and fractionation techniques”, Environ. Chem., 8, 2, 2011, 155-162, DOI: 10.1071/EN10119.

BREWER P.J., STOICA D. et BROWN R.J.C., “Sensitivities of key parameters in the preparation of silver/silver chloride electrodes used in Harned cell measurements of pH”, Sensors, 11, 8, 2011, 8072-8084, DOI: 10.3390/s110808072.

DELATOUR V., LALÈRE B., DE GRAEVE J. et VASLIN-REIMANN S., “Developpement of reference methods for the measurement of biomarkers in France”, Ann. Biol. Clin., 68, 6, 2010, 698-699.

DELATOUR V., LALÈRE B., DUMONT G., HATTCHOUEL J.-M., FROISSART M., DE GRAEVE J. et VASLIN-REIMANN S., “Development of a reference method for creatinine measurement to improve diagnosis and follow-up of kidney disease”, Revue française de métrologie, 26, 2011, 21-31, DOI: 10.1051/rfm/2011008.

JITARU P., OSTER C., LABARRAQUE G., VASLIN-REIMANN S. et FISICARO P., “A metrological approach for the determination of selenium status in human serum”, Accred. Qua.l Assur., 16, 11, 2011, 545-552, DOI: 10.1007/s00769-011-0815-9.

PIERONI L., DELANEY P., BOUTTEN A., BARGNOUX A.-S., ROZET E., DELATOUR V., CARLIER M.-C., HANSER A.-M., CAVALIER E., FROISSART M. et CRISTOL J.-P., “A multicentric evaluation of IDMS-traceable creatinine enzymatic assays”, Clinica Chimica Acta, 412, 23-24, 2011, 2070-2075, DOI: 10.1016/j.cca.2011.07.012.

SCHIEL D., RIENITZ O., JAHRLING R., GUETTLER B., MATSCHAT R., SCHARF H., BIRKHAHN J., LABARRAQUE G., FISICARO P., BORCHERS U. et SCHWESIG D., “Metrological concept for comparable measurement results under the European water framework directive: demonstration of its applicability in elemental analysis”, Accred. Qual. Assur., 16, 10, 2011, 489-498, DOI: 10.1007/s00769-011-0792-z.

SPITZER P., ADEL B., MEYER J., MATZKE J., GONZAGA F., BORGES P., DIAS J., HONGYU X., BING W., JAKOBSEN P., CHAMPION R., OHATA M., MAKSIMOV I., HIOKI A., VYSKOCIL ., MARIASSY M. et PRATT K., “Final report on CCQM-K19.1 - ph of borate buffer”, Metrologia, 48, Techn. Suppl., 2011, 08010, 1-22.

SPITZER P., FISICARO P., MEINRATH G. et STOICA D., “pH buffer assessment and Pitzer’s equations”, Accred. Qua.l Assur., 16, 4-5, 2011, 191-198, DOI: 10.1007/s00769-010-0743-0.

STOICA D., BREWER P.J., BROWN R.J.C. et FISICARO P., “Influence of the preparation method on the electrochemical behaviour of Ag/AgCl reference electrodes”, Electrochimica Acta, 56, 27, 2011, 10009-10015, DOI: 10.1016/j.electacta.2011.08.089.

STOICA D., YARDIN C., VASLIN-REIMANN S. et FISICARO P., “Evaluation of standard potential of Ag/AgCl electrode in a 50 wt% water-ethanol mixture”, Journal of Solution Chemistry, 40, 11, 2011, 1819-1834, DOI: 10.1007/s10953-011-9758-3.

Communications

ALASONATI E., “Evaluation of the measurement uncertainties for multiple-spiking isotope dilution procedures”, European Winter Conference on Plasma Spectrochemistry 2011, Saragosse, Espagne, 30 janvier - 3 février 2011.

CHAMPION R., GUIGUES N., GHESTEM J.-P., et  LEPOT B., “In-situ inter-laboratory comparisons on physico-chemical parameters: a collaborative study”, IMEKO TC Conference (TC8 - TC23 - TC24) “Metrological traceability in the globalisation age”, Paris, France, 6-8 avril 2011.

DELATOUR V., LALÈRE B. et VASLIN-REIMANN S., “Development of reference methods for the measurement of biomarkers”, IMEKO TC Conference (TC8 - TC23 - TC24) “Metrological traceability in the globalisation age”, Paris, France, 6-8 avril 2011.

FISICARO P. et VASLIN-REIMANN S., “Metrology for biofuels”, IMEKO TC Conference (TC8 - TC23 - TC24) “Metrological traceability in the globalisation age”, Paris, France, 6-8 avril 2011.

FRAISSE P.O., LECLERC O., LABARRAQUE G., FISICARO P. et OSTER C., “Method developement for the accurate quantification of genomic DNA Legionella Pneumophila”, Congrès IMEKO - Metrological traceability in the globalisation age, Paris, France, 8 avril 2011.

GUIGUES N., CHAMPION R., LACHENAL J. et HANCE E., “Metrological characterisation and traceability of in situ probes for continuous water quality monitoring: a case study”, IMEKO TC Conference (TC8 - TC23 - TC24) “Metrological traceability in the globalisation age”, Paris, France, 6-8 avril 2011.

LARDY-FONTAN S., CABILLIC J., PEIGNAUX M., STUMPF C., LEPOT B., LEOZ E., MIEGE C. et LALÈRE B., “The usefulness of assignation of reference values in inter laboratories comparisons French demonstrations in the field of environmental survey”, IMEKO TC Conference (TC8 - TC23 - TC24) “Metrological traceability in the globalisation age”, Paris, France, 6-8 avril 2011.

LARDY-FONTAN S., CAURANT A., SUTOUR CH., LALÈRE B., MACÉ T. et VASLIN–REIMAN S., “Certified Reference Material as a key for QA/QC. Assessment of the performance of seven French laboratories for the analysis of BTEX loaded on passive samplers through a proficiency testing”, International Passive Sampler Workshop (IPSW), Cracovie, Pologne, 11-14 mai 2011.

ALASONATI E., LABARRAQUE G. et FISICARO P., “Tributyltin: not a novel contaminant but a present-day challenge”, EuCheMS International Conference on Chemistry and the Environment, Zurich, Suisse, 14 septembre 2011.

CABILLIC J., PHILIPP R., SCHIEL D., EMTEBORG H., GOENANA-INFANTE H. et LALÈRE B., “Joint Research Project ENV08 “Traceable measurements for monitoring critical pollutants under the European Water Framework Directive (WFD) 2000/60/EC”, 15e Congrès international de métrologie, Paris, France, 3-6 octobre 2011.

HEUILLET M., DELATOUR V., LALERE B. et VASLIN-REIMANN S., “How to perform traceable measurements for biomarkers quantification”, 15e Congrès international de métrologie, Paris, France, 3-6 octobre 2011.

STOICA D. et FISICARO P., “Determination of standard pH values for reference potassium hydrogen phtalates buffer solutions in water-ethanol mixture (50 wt%)”, 15e Congrès international de métrologie, Paris, France, 3-6 octobre 2011.

Publications and communications in the field of "Amount of substance and chemistry" by authors of the French metrology network in 2012

Publications

BARBE J., DIJOUX F., YARDIN C. et MACÉ T., “Measurement of Helium micro-flows for gas chromatography by the dilution method”, MAPAN-Journal of Metrology Society of India, 27, 2, 2012, 77-81, DOI: 10.1007/s12647-012-0015-z.

DELATOUR V., LALÈRE B., SAINT-ALBIN K., PEIGNAUX M., HATTCHOUEL J.-M., DUMONT G., DE GRAEVE J., VASLIN-REIMANN S. et GILLERY P., “Continuous improvement of medical test reliability using reference methods and matrix-corrected target values in proficiency testing schemes: Application to glucose assay”, Clinica Chimica Acta, 413, 23-24, 2012, 1872-1878, DOI: 10.1016/j.cca.2012.07.016.

HAUSWALDT A.-L., RIENITZ O., JÄHRLING R., FISCHER N., SCHIEL D., LABARRAQUE G. et MAGNUSSON B., “Uncertainty of standard addition experiments: a novel approach to include the uncertainty associated with the standard in the model equation”, Accreditation and Quality Assurance, 17, 2, 2012, 129-138, DOI: 10.1007/s00769-011-0827-5.

HEUILLET M., LALÈRE B., PEIGNAUX M., DE GRAEVE J., VASLIN-REIMANN S., PAIS DE BARROS J., GAMBERT P., DUVILLARD L et DELATOUR V., “Validation of a reference method for total cholesterol measurement in human serum and assignation of reference values to proficiency testing samples”, Clinical Biochemistry, 46, 4–5, 2012, 359-364, DOI: 10.1016/j.clinbiochem.2012.11.026.

MIEGE C., MAZELLA N., SCHIAVONE S., DABRIN A., BERHO C., GHESTEM J.-P., GONZALEZ C., GONZALEZ J.-L., LALÈRE B., LARDY-FONATN S., LEPOT B., MUNARON D., TIXIER C. et COQUERY M., “An in situ intercomparison exercise on passive samplers for the monitoring of metals polyclic aromatic hydrocarbons and pesticides in surface water”, Trends in Analytical Chemistry, 36, 2012, 128-143, DOI: 10.1016/j.trac.2012.01.009.

SWART C., FISICARO P., GOENAGA-INFANTEC H. et ZAKELD S., “Metalloproteins – a new challenge for metrology”, Metallomics, 4, 2012, 1137-1140, DOI: 10.1039/C2MT90049A.

VIALLON J., MOUSSAY P., IDREES F., WIELGOSZ R., MACÉ T., COUETTE J., “Final report, ongoing key comparison BIPM.QM-K1: Ozone at ambient level, comparison with LNE”, Metrologia, 49, 1A, 2012, DOI: 10.1088/0026-1394/49/1A/08012.

WESTWOOD S., JOSEPHS R., CHOTEAU T., DAIREAUX A., MESQUIDA C., WIELGOSZ R., ROSSO A., RUIZ DE ARECHAVALETA M., DAVIES S., WANG H., PIRES DO REGO E.C., MARQUES RODRIGUES J., DE FREITAS GUIMARÃES E., VINICIUS BARRETO SOUSA M., MONTEIRO T.M., DAS NEVES VALENTE L.A., MARQUES VIOLANTE F.G., RIBEIRO ALMEIDA R.R., BAPTISTA QUARESMA M.C., NOGUEIRA R., WINDUST A., DAI X., LI X., ZHANG W., LI M., SHAO M., WEI C., WONG S.-K., CABILLIC J., GANTOIS F., PHILIPP R., PFEIFER D., HEIN S., KLYK-SEITZ U.-R., ISHIKAWA K., CASTRO E., GONZALEZ N., KRYLOV A., LIN T.T., KOOI L.T., FERNANDES-WHALEY M., PRÉVOO D., ARCHER M., VISSER R., NLHAPO N., DE VOS B., AHN S., POOKROD P., WIANGNON K., SUDSIRI N., MUAKSANG K., CHERDCHU C., GÖREN A.C., BILSEL M., LE GOFF T., BEARDEN D., BEDNER M., DUEWER D., HANCOCK D., LANG B., LIPPA K., SCHANTZ M. et SIEBER J., “Final report on key comparison CCQM-K55.b (aldrin): An international comparison of mass fraction purity assignment of aldrin”, Metrologia, 49, 1A, 2012, 128-143, DOI: 10.1088/0026-1394/49/1A/08014.

Communications

STOICA D., “Definition and standards for seawater pH measurements”, Workshop “Standards for Ocean measurements”, Warnemünde, Allemagne, 24 janvier 2012.

GUIGUES N., CHAMPION R., ALASONATI E. et HANCE E., “Traceability and estimation of uncertainty for in situ probes for continuous water quality monitoring: a case study”, Measurement Traceability for Water Sensors (SWIG), Teddington, Royaume-Uni, 16 mai 2012.

FAVRE G. et VASLIN-REIMANN S., « Les activités du LNE dans le domaine de la métrologie en chimie », Journée d’inauguration du DIM Analytics, Saclay, France, 4 juin 2012.

GUIGUES N., DESENFANT M. et HANCE E., “Assessing sampling contribution to measurement uncertainty for a selection of water quality parameters: a case study”, Analytical Days, Uppsala, Suède, 11–13 juin 2012.

LARDY-FONTAN S., GUIGUES N., ALASONATI E., CHAMPION R., ABERT S., MANSUIT P. et HANCE E., “Deployment of passive samplers for routine monitoring at a small catchment in the North Eastern part of France: optimisation of deployment conditions and technology transfer to a routine laboratory”, 5th International Passive Sampling Workshop and Symposium (IPSW 2012), Columbia, États-Unis d’Amérique, 11–12 septembre 2012.

DELATOUR V., HEUILLET M., PEIGNAUX M., LALERE B. et VASLIN-REIMANN S., « Apport de la spectrométrie de masse et des méthodes de référence pour le contrôle qualité en biologique clinique », 29es Journées Françaises de Spectrométrie de Masse, Orléans, France, 17–20 septembre 2012.

HEUILLET M., DELATOUR V., PEIGNAUX M., LALERE B., DE GRAEVE J., VASLIN-REIMANN S. et DUVILLARD L., « Développement et validation d’une méthode de référence pour le dosage du cholestérol total et application au contrôle qualité en biologie clinique », 29es Journées Françaises de Spectrométrie de Masse, Orléans, France, 17–20 septembre 2012.

LARDY-FONTAN S., LE DIOURON V., LALERE B. et VASLIN-REIMANN S., “Improvement of the reliability of quantitative analysis by liquid chromatography-mass spectrometry, the weight of the calibration and the method of quantification – A demonstration on multiresidues analysis of pesticides at ultra-traces level in environmental matrices”, 29es Journées Françaises de Spectrométrie de Masse, Orléans, France, 17–20 septembre 2012.

GUIGUES N., ALASONATI E., CHAMPION R. et HANCE E., “Metrological characterization of sensors for continuous water quality measurement”, Environmental Sensors 2012, Biarritz, France, 23–28 septembre 2012.

DELATOUR V., PEIGNAUX M., LALERE B. et VASLIN-REIMANN S., « Caractérisation et quantification de peptides pour la protéo-mique quantitative », Adebiotech, Paris, France, 3 octobre 2012.

GRATIA A., MERLET D., LE DIOURON V., DUCRUET V. et LYATHAUD C., “A new method to assess the composition of food contact biobased materials by mass spectrometry and NMR”, 5th International Symposium on Food Packaging, Berlin, Allemagne, 14–16 novembre 2012.

VASLIN-REIMANN S. et DELATOUR V., « Matériaux de Référence Certifiés pour la biologie médicale : une denrée rare en France ? », Journée Technique du Collège Français de Métrologie, Paris, France, 27 novembre 2012.

BRIEUDES V., LARDY-FONTAN S., LALÈRE B. et BUDZINSKI H., “Monitoring strategy for relevant psychotropic substances and metabolites in the French aquatic system”, Occurrence, fate and effects of emerging pollutants in the environment – Chemical analysis and toxicological assessment, Amsterdam, Pays-Bas, 29–30 novembre 2012.

CHAMPION R. et BOTHOREL L., « Travaux sur les référentiels et la traçabilité dans le domaine de l’environnement et de la qualité », Salon Pollutec, Lyon, France, 30 novembre 2012.

Publications and communications in the field of "Amount of substance and chemistry" by authors of the French metrology network in 2013

Publications

BAUME M., GARRELLY L., FACON J.-P., BOUTON S., FRAISSE P.-O., YARDIN C., REYROLLE M. et JARRAUD S., “The characterization and certification of a quantitative reference material for Legionella detection and quantification by qPCR”, Journal of Applied Microbiology, 114, 6, 1725-1733, 2013, DOI: 10.1111/jam.12172.

BOUTTEN A., BARGNOUX A.S., CARLIER M.C., DELANAYE P., ROZET E., DELATOUR V., CAVALIER E., HANSER A.M., FROISSART M., CRISTOL J.-P. et PIÉRONI L., “Enzymatic but not compensated Jaffe methods reach the desirable specifications of NKDEP at normal levels of creatinine. Results of the French multicentric evaluation”, Clinica Chimica Acta, 419, 2013, 132-135, DOI: 10.1016/j.cca.2013.01.021.

FLAMANT M., VIDAL-PETIOT E., METZGER M., HAYMANN J.P., LETAVERNIER E., DELATOUR V., KARRAS A., THERVET E., BOFFA J.J., HOUILLIER P., STENGEL B., VRTOVSNIK F. et FROISSART M., “Performance of GFR Estimating Equations in African Europeans: Basis for a Lower Race-Ethnicity Factor Than in African Americans”, Am. J. of Kidney Disease, 62, 1, 2013, 182-184, DOI: 10.1053/j.ajkd.2013.03.015.

GUIGUES N., DESENFANT M. et HANCE E., “Combining multivariate statistics and analysis of variance to redesign a water quality monitoring network”, Environmental Science: Process & Impacts, 15, 2013, 1692-1705, DOI: 10.1039/c3em00168g.

LECLERC O., FRAISSE P.-O., LABARRAQUE G., OSTER C., PICHAUT J.-P., BAUME M., JARRAUD S., FISICARO P. et VASLIN-REIMANN S., “Method development for genomic Legionella pneumophila DNA quantification by inductively coupled plasma mass spectrometry”, Analytical Biochemistry, 435, 2, 153-158, 2013, DOI: 10.1016/j.ab.2012.12.023.

SPITZER P., BASTKOWSKI F., ADEL B., DIMITROVA L., GONZAGA F.B., FISICARO P. et STOICA D., “Final report on CCQM-K91: Key comparison on pH of an unknown phthalate buffer”, Metrologia, 50, 1A, 2013, DOI: 10.1088/0026-1394/50/1A/08016.

Communications

CHEBIL S., CHAMPION R., FAURE P., FISICARO P., MOIROUX L. et MONOD M.O., « Nouveau capteur de pH pour l'analyse de l'eau », 6e Colloque Interdisciplinaire en Instrumentation, Lyon, France, 29–30 janvier 2013.

LALERE B., LARDY-FONTAN S., CABILLIC J., LEDIOURON V. et PEIGNAUX M., « Méthodologie et métrologie pour l’acquisition de mesures quantitatives fiables à l’état traces dans l’environnement », Colloque du DIM Analytics, Paris, France, 18–19 avril 2013.

MOTZKUS C., GAIE-LEVREL F., IDRAC J., OSTER D., MACE T. et VASLIN-REIMANN S., « Développement d’une méthodologie métrologique pour la caractérisation physico-chimique de poudres nanostructurées », Colloque du DIM Analytics, Paris, France, 18–19 avril 2013.

MACE T., SUTOUR C. et KAISER C., “Measurement methods for zero gases”, MACPoll Workshop on “Zero Gases”, Delft, Pays-Bas, 4 juin 2013.

MACE T., SUTOUR C. et COUETTE J., “Calibration gases for existing air quality directive pollutants at limit values”, GAS2013, Rotterdam, Pays-Bas, 5–7 juin 2013.

JITARU P., OSTER C., LABARRAQUE G., DEL CASTILLO M.E., VASLIN-REIMANN S. et FISICARO P., “A comparison of conventional (off-line) and on-line isotope dilution ICP-MS for the determination of total Selenium in human serum”, XXXVIII Colloquium Spectroscopicum Internationale, Tromsø, Norvège, 17–20 juin 2013.

GUIGUES N., LARDY-FONTAN S., ALASONATI E., CHAMPION R., CABILLIC J., ABERT S., LE FAHLER H., EYL D., ENGLES X., MANSUIT P. et HANCE E., “Implementation of SPMD and DGT for routine water quality monitoring at the long-term Observatory of the Environment (OPE) in the North Eastern part of France”, 6th International Passive Sampling Workshop and Symposium, Bordeaux, France, 26–29 juin 2013.

LARDY-FONTAN S., GUIGUES N. et LALERE B., “How to make reliable passive samplers measurements for water monitoring ?”, 6th International Passive Sampling Workshop and Symposium, Bordeaux, France, 26–29 juin 2013.

TIXIER C., BERHO C., LARDY– FONTAN S., LEPOT B., BUDZINSKI H., ALLAN I., CHHIM N., DYMOND P., GONZALEZ C., GRAVELL A., GUNOLD R., LLORCA J., LOHMANN R., LORGEOUX C., MARRUCCI A., PAVONIC M., PEINERUD E., RUMNEY H., SMEDES F., UHER E., VRANA B. et MIÈGE C., “AQUAREF intercomparison passive sampling exercise: Monitoring of Polycyclic Aromatic Hydrocarbons (PAHs)”, 6th International Passive Sampling Workshop and Symposium, Bordeaux, France, 26–29 juin 2013.

FISICARO P. et DEL CASTILLO M.E., “Metrology for Metalloproteines”, Franco-Japanese Workhop on Metallomics, Pau, France, 6–7 juillet 2013.

CHEBIL S., CHAMPION R., FAURE P., FISICARO P. et MONOD M.O., « Nouveau capteur de pH pour l'analyse de l'eau », Journées d'Electrochimie (JE 2013), Paris, France, 8–11 juillet 2013.

DEL CASTILLO M.E., OSTER C., LABARRAQUE G., JITARU P., GOENAGA-INFANTE H. et FISICARO P., “Low level determination of selenomethionine in human serum by double species-specific isotope dilution HPLC-ICP-MS: The importance of blank quantification”, 4th International Symposium on Metallomics, Oviedo, Espagne, 8–11 juillet 2013.

STOICA D., BROWN R.J.C., SPITZER P., CHAMPION R. et FISICARO P., « Fiabilité des mesures dans les milieux à matrices complexes : Les solutions tampon disponibles sur le marché sont-elle adaptées ? », Journées d'Electrochimie (JE 2013), Paris, France, 8–11 juillet 2013.

SWART C., ZAKE S., FISICARO P. et GOENAGA-INFANTE H., “Can physicians really rely on laboratory diagnostics?”, 4th International Symposium on Metallomics, Oviedo, Espagne, 8–11 juillet 2013.

DELATOUR V., “Development of new reference methods and standards for advanced lipoprotein testing: is measurement traceability achievable ?”, Annual meeting of American Association for Clinical Chemistry, Houston, Etats-Unis, 28 juill.–1er août 2013.

HEUILLET M., PEIGNAUX M., LALERE B., VASLIN-REIMANN S., DUVILLARD L. et DELATOUR V., “A commutability study coupled to a multicentric analysis of accuracy of total cholesterol, LDL-C, HDL-C and total glycerides assays”, Annual meeting of American Association for Clinical Chemistry, Houston, Etats-Unis, 28 juill.–1er août 2013.

STOICA D., ADEL B., ASAKAI T., BREWER P.J., BROWN R.J.C., CAMÕES M.F., DIAS F.A., FERRARA E., FILIPE E., FISICARO P., HIOKI A., MAKSIMOV I., MÁRIÁSSY M., OLIVEIRA C., SPITZER P., BENACHOUR M. et TROIA A., “pH measurements in seawater: Reducing the limitations of the existing primary standard buffers”, 16th International Conference on the Properties of Water and Steam, Londres, Royaune-Uni, 1–5 septembre 2013.

RAAB A., GOENAGA-INFANTE H., DEL CASTILLO M.E., FISICARO P., KONOPKA A. et LEHMANN W.D., “Quantification of Selenoproteins: the need for reference materials, methods and standards (focus on SEPP1)”, 10th International Symposium on Selenium in Biology and Medicine 2013, Berlin, Allemagne, 14–18 septembre 2013.

BARBE J., DIJOUX F. et MACÉ T., “Development of a gas micro flow transfer standard”, 16th International Flow Measurement Conference (Flomeko 2013), Paris, France, 24–26 septembre 2013.

BARBE J., DIJOUX F. et MACÉ T., “National gas low flow standards and calibration services at LNE”, 16th International Flow Measurement Conference (Flomeko 2013), Paris, France, 24–26 septembre 2013.

CHAMPION R., FISICARO P., STOICA D. et VASLIN-REIMANN S., « Vers une meilleure traçabilité des mesures électrochimiques », 16e Congrès International de Métrologie, Paris, France, 7–10 octobre 2013.

MACE T., SUTOUR C. et COUETTE J., “Calibration gases for existing air quality directive pollutants at limit values”, 16th International Flow Measurement Conference (Flomeko 2013), Paris, France, 24–26 septembre 2013.

SWART C., ZAKE S., FISICARO P. et GOENAGA-INFANTE H., “Metrological approach for the quantification of metalloproteins”, 16th International Flow Measurement Conference (Flomeko 2013), Paris, France, 24–26 septembre 2013.

CABILLIC J., HEIN S., LEHNIK-HABRINK P., CALABRETTA E., POTALIVO M., BELLI M., BILSEL M., GOKÇEN T., CEYHAN GOREN A., CRINA I., BUZUIANU M., LALERE B. et PHILIPP R., “Joint Research Project ENV08 : Traceable measurements for monitoring critical pollutants under the European Water Framework Directive (WFD) 2000/60/EC”, 16e Congrès International de Métrologie, Paris, France, 7–10 octobre 2013.

DELATOUR V., HEUILLET M., LALERE B. et VASLIN-REIMANN S., « Production d’un matériau de référence certifié pour le glucose, la créatinine et le cholesterol total et organisation d’une étude de commutabilité couplée à une étude multicentrique de la justesse des dosages de routine », 16e Congrès international de métrologie, Paris, France, 7–10 octobre 2013.

LARDY-FONTAN ., GUIGUES N., LALERE B. et VASLIN-REIMANN S., “Metrological needs for monitoring aquatic environments: from the demonstration of metrological traceability to the decision making process”, 16e Congrès International de Métrologie, Paris, France, 7–10 octobre 2013.

MOTZKUS C., GAIE-LEVREL F., MACE T. et VASLIN-REIMANN S., « Travaux prénormatifs sur la caractérisation des nanoparticules dans l’air », Séminaire CETAMA, Tours, France, 16 octobre 2013.

MACÉ T., SUTOUR C. et COUETTE J., “Results of the comparison exercise of NO, NO2 and SO2 at LVs”, Workshop MACPoll, Ispra, Italie, 19 novembre 2013.

Publications and communications in the field of "Amount of substance and chemistry" by authors of the French metrology network in 2014

Publications

ALASONATI E., FABBRI B., FETTIG I., YARDIN C., DEL CASTILLO BUSTO M., RICHTER J., PHILIPP R. et FISICARO P., Experimental design for TBT quantification by isotope dilution SPE-GC-ICP-MS under the European Water Framework Directive”, Talanta, 134, 2015, 576-586, DOI: 10.1016/j.talanta.2014.11.064.

CHEBIL S., FISICARO P. et MONOD M.-O., Direct electrochemical synthesis and characterization of polypyrrole nano- and micro-snails”, Electrochimica Acta, 123, 2014, 527-534, DOI: 10.1016/j.electacta.2014.01.058.

CHEBIL S., FISICARO P., MONOD M.-O. et CHAMPION R., « Nouveau capteur de pH pour l’analyse de l’eau », Instrumentation & Interdisciplinarité – Capteurs Chimiques & Physiques, Editions EDP Sciences, 2014, 381-386, ISBN : 978-2-7598-1116-8.

DA G., GEHIN E., BEN-OTHMANE M., HAVET M., SOLLIEC C. et MOTZKUS C., An experimental approach to measure particle deposition in large circular ventilation duc”, Environmental Science and Pollution Research, 22, 7, 2014, 4873-4880, DOI: 10.1007/s11356-014-2859-y.

ELORDUI-ZAPATARIETXE S., FETTIG I., PHILIPP R., GANTOIS F., LALÈRE B., SWART C., PETROV P., GOENAGA-INFANTE H., VANERMEN G., BOOM G. et EMTEBORG H., “Novel concepts for preparation of reference aterials as whole water samples for priority substances at ng.L-1 level using model uspended particulate matter and humic”, Analytical and Bioanalytical Chemistry, 2014, DOI: 10.1007/s00216-014-8349-8.

HODOROABA V.-D., MOTZKUS C., MACÉ T. et VASLIN-REIMANN S., Performance of High-Resolution SEM/EDX Systems Equipped with Transmission Mode (TSEM) for Imaging and Measurement of Size and Size Distribution of Spherical Nanoparticles”, Microscopy and Microanalysis, 20, 2, 2014, 602-612, DOI: 10.1017/S1431927614000014.

LARDY-FONTAN S., GUIGUES N., LALÈRE B. et VASLIN-REIMANN S., “Metrological needs for monitoring aquatic environments: From the demonstration of metrological traceability to the decision making process”, EPJ Web of Conferences, 77, 2014, DOI: 10.1051/epjconf/20147700011.

MOTZKUS C., GAIE-LEVREL F., AUSSET P., MAILLÉ M., BACCILE N., VASLIN-REIMANN S., IDRAC J., OSTER D., FISCHER N. et MACÉ T., Impact of batch variability on physicochemical properties of manufactured TiO2 and SiO2 nanopowders”, Powder Technology, 267, 2014, 39-53, DOI: 10.1016/j.powtec.2014.06.055.

MOTZKUS C., GAIE-LEVREL F., MACE T., DELVALLEE A., DUCOURTIEUX S., MICHIELSEN N., BONDIGUEL S., GENSDARMES F., AUSSET P., MAILLE M. et VASLIN-REIMANN S., « Travaux prénormatifs sur la caractérisation de la taille des nanoparticules dans l’air : comparaison inter laboratoires avec des techniques de mesure directes et indirectes », Spectra Analyse, 296, 2014.

OSTER C., LABARRAQUE G. et FISICARO P., Certification of a reference material of metal content in atmospheric particles loaded on filters”, Analytical and Bioanalytical Chemistry, 2014, DOI: 10.1007/s00216-014-8194-9.

STOICA D., BEN-ACHOUR M., SPITZER P., FISICARO P. et VASLIN-REIMANN S., « Mesures du pH de l’eau de mer : un défi d’actualité », Revue Française de Métrologie, 34, 2014, 23-30, DOI: 10.1051/rfm/2014006.

SWART C., ZAKEL S., FRANK C., FISICARO P. et GOENAGA-INFANTE H., “Metrological approach for the quantification of metalloproteins (EMRP project HLT05)”, EPJ Web of Conferences, 77, 2014, DOI: 10.1051/epjconf/20147700007.

WESTWOOD S., JOSEPHS R., GANTOIS F., LALÈRE B., SCHANTZ M.M. et SIEBER J.R., “Final report on key comparison CCQM-K55.c (L-(+)-Valine): Characterization of organic substances for chemical purity”, Metrologia, 51, 1A, 2014, DOI: 10.1088/0026-1394/51/1A/08010.

Communications

MACÉ T., MACPoll intercomparison results for NOx and SO2 at EU limit values”, EURAMET-METCHEM Gas Sub-Committee, Teddington, Angleterre, 5 février 2014.

VASLIN-REIMANN S., « Améliorer la qualité des résultats de mesure: le rôle de la métrologie », Colloque DIM ANALYTICS 2014: Défis analytiques et société, Paris, France, 8 avril 2014.

FETTIG I., RICHTER J., PHILIPP R., PIECHOTTA C., ALASONATI E., FABBRI B. et FISICARO P., Optimizing of a solid phase extraction method for tributyltin using a design of experiment and quantification with ID-GC-ICP-MS”, SETAC Europe 24th Annual Meeting, Bâle, Suisse, 11-15 mai 2014.

LARDY-FONTAN S., BRIEUDES V., LAVISON-BOMPARD G., CANDIDO P., COUTURIER G., BUDZINSKI H. et LALÈRE B., Implementation of a complementary monitoring strategy to enable an efficient survey of pharmaceuticals in urban water cycle. A case study on the parisian area”, SETAC Europe 24th Annual Meeting, Bâle, Suisse, 11-15 mai 2014.

LARDY-FONTAN S., LAVISON-BOMPARD G., BRIEUDES V., CANDIDO P., COUTURIER G., LALÈRE B. et BUDZINSKI H., From the initial monitoring to thedevelopment of a reference method. A case study on pharmaceuticals residues on the Paris area”, SETAC Europe 24th Annual Meeting, Bâle, Suisse, 11-15 mai 2014.

KAISER C., SUTOUR CH. et MACÉ T., Development of a quad quantum cascade laser spectrometer for simultaneous detection of NO, NO2, SO2 and CO at nmol/mol levels, data processing and associated uncertainties”, MacPoll final conference, Delft, Pays-Bas, 13-14 mai 2014.

MACÉ T., Validation of the methods used for generating standard gas mixtures by an interlaboratory comparison for NO, NO2 and SO2 at limit values”, MacPoll final conference, Delft, Pays-Bas, 13-14 mai 2014.

FISICARO P., « Améliorer la qualité des résultats de mesure : le rôle du laboratoire national de métrologie », Spectr'Atom 2014, Pau, France, 20-23 mai 2014.

PALOS M., DEL CASTILLO E., PANNIER F. et FISICARO P., « Détermination des métalloprotéines par DI-ICPMS afin d'assurer la traçabilité métrologique en biochimie clinique », Spectr'Atom 2014, Pau, France, 20-23 mai 2014.

BROS P., BARTHELEMY N., VIALARET J., BECHER F., GABELLE A., DELATOUR V., LEHMANN S. et HIRTZ C., Mass spectrometry quantification of human CSF Tau protein in sub-nanogram/milliliters range”, 12e journée de l’Ecole Doctorale CBS2, Montpellier, France, Mai 2014.

BROS P., BARTHELEMY N., VIALARET J., BECHER F., GABELLE A., DELATOUR V., LEHMANN S. et HIRTZ C., Comparison of PRM and SRM analytical performances for the quantification of Tau protein in human C”, SMAP 2014 : Congrès français de Spectrométrie de Masse et d’Analyse Protéomique, Lyon, France, juin 2014.

ALASONATI E., FETTIG I., FABBRI B., YARDIN C., RINCEL A., DEL CASTILLO M.E., PANAYOT P., PHILIPP R. et FISICARO P., TBT quantification by isotope dilution mass spectrometry under the European water framework Directive”, International Symposium on Environmental Analytical Chemistry (ISEAC38), Lausanne, Suisse, 16-19 juin 2014.

KOTZEVA B., ALASONATI E., PHILIPP R. et FISICARO P., Development of analytical method for TBT speciation in coastal lyes and sea water (Pomorie Lake, Black Sea, Bulgaria)”, International Symposium on Environmental Analytical Chemistry (ISEAC38), Lausanne, Suisse, 16-19 juin 2014.

LARDY-FONTAN S., LAVISON-BOMPARD G., BRIEUDES V., CANDIDO P., COUTURIER G., LALÈRE B. et BUDZINSKI H., Measurement uncertainty in water monitoring: contribution of both laboratory and sampling uncertainties. A cases study on pharmaceuticals in the Seine River (France)”, International Symposium on Environmental Analytical Chemistry (ISEAC38), Lausanne, Suisse, 16-19 juin 2014.

LAVISON-BOMPARD G., LARDY-FONTAN S., BRIEUDES V., CANDIDO P., JOYEUX M., LALÈRE B. et BUDZINSKI H., Implementation of complementary monitoring strategies for an effective survey of psychotropic drugs and metabolites in drinking water treatment plants in the parisian area”, International Symposium on Environmental Analytical Chemistry (ISEAC38), Lausanne, Suisse, 16-19 juin 2014.

RAAB A., FELDMAN J., GOENAFA-INFANTE H., NUNNEZ S., DEL CASTILLO M.E., FISICARO P., KONOPKA A. et LEHMANN W.-D., Determination of Selenoprotein P in human serum by isotope dilution ICP-MS”, THE BNASS / TraceSpec Tandem Conference, Aberdeen, Royaume-Uni, 31 août-04 sept. 2014.

VASLIN-REIMANN S. et DELATOUR V., « Quelles recherches pour progresser dans la maîtrise des analyses? », JT du CFM, Paris, France, 23 septembre 2014.

LAVISON-BOMPARD G., BRIEUDES V., LARDY-FONTAN S., CANDIDO P., COUTURIER G., LALERE B., JOYEUX M. et BUDZINSKI H., « Deux stratégies d’échantillonnage pour la surveillance de la qualité des eaux des usines de potabilisation d’Eau de Paris vis-à-vis de substances pharmaceutiques par des résidus médicamenteux », JIE 2014, Poitiers, France, 4-6 novembre 2014.

VASLIN-REIMANN S. et LALERE B., « Traçabilité des analyses Chimiques », JT du CFM, Paris, France, 10 décembre 2014.

ALASONATI E., DEL CASTILLO M.E., LABARRAQUE G. et FISICARO P., Speciation analyses: applications to metalloproteins and persistent pollutants”, CETAMA GT 12 – ICP/MS, Les Renadières, France.

Publications and communications in the field of "Amount of substance and chemistry" by authors of the French metrology network in 2015

Publications

ALASONATI E., FABBRI B., FETTIG I., YARDIN C., DEL CASTILLO BUSTO M.-E., RICHTER J., PHILIPP R. et FISICARO P., “Experimental design for TBT quantification by isotope dilution SPE_GC_ICP_MS under the European water framework directive”, Talanta, 134, 2015, 576-586, DOI: 10.1016/j.talanta.2014.11.064.

BARBE J., BOINEAU F., MACÉ T. et OTAL P., “Development of a gas micro flow transfer standard”, Flow measurement & instrumentation, numéro spécial, 44, 2015, 43-50, DOI: 10.1016/j.flowmeasinst.2014.11.011.

BENKOULA S., SUBLEMONTIER O., PATANEN M., NICOLAS C., SIROTTI F., NAITABDI A., GAIE-LEVREL F., ANTONSSON E., AUREAU D., OUF F-X., WADA S-I., ETCHEBERRY A., UEDA K. et MIRON C., “Water adsorption on TiO2 surfaces probed by soft X-ray spectroscopies: Bulk materials vs. isolated nanoparticles”, Scientific Reports, 5, 15088, 2015, DOI: 10.1038/srep15088.

BREWER P.J., PANAGOULIA D., BROWN R.J.C., TROMANS A., REYES A., ARCE M., SPITZER P., FISICARO P. et STOICA D., “International comparison on Ag|AgCl electrodes for pH measurement”, Measurement, 66, 2015, 131-138, DOI: 10.1016/j.measurement.2015.01.029.

BROS P., VIALARET J., BARTHELEMY N., DELATOUR V., GABELLE A., LEHMANN S. et HIRTZ C., “Antibody-free quantification of seven tau peptides in human CSF using targeted mass spectrometry”, Frontiers in Neuroscience, 9, 2015, 302, 1-8, DOI: 10.3389/fnins.2015.00302.

BROS P., DELATOUR V., VIALARET J., LALERE B., BARTHELEMY N., GABELLE A., LEHMANN S. et HIRTZ C., “Quantitative detection of amyloidbetapeptides by mass spectrometry: state of the art and clinical applications”, Clinical Chemistry and Laboratory Medicine (CCLM), 53, 10, 2015, 1483-1493, DOI: 10.1515/cclm-2015-099.

BROWN R.J.C., BREWER P.J., ENT H., FISICARO P., HORVAT M., KIM K-H. et QUETEL C.R., “Who should take responsibility for decisions on internationally recommended datasets? The case of the mass concentration of mercury in air at saturation”, Metrologia, 52, 5, 2015, L25-L30, DOI: 10.1088/0026-1394/52/5/L25.

CABILLIC J., FALLOT C., HEIN S., LALERE B. et PHILIPP R., « Développement et validation d’une méthode de référence pour l’analyse des HAP dans l’eau totale dans le contexte de la DCE », Revue française de métrologie, 40, 2015, 3-12, DOI: 10.1051/rfm/2015014.

CHIVAS-JOLY C., LONGUET C., MOTZKUS C. et LOPEZ CUESTA J-M., “Influence of the composition of PMMA nanocomposites on gaseous effluents emitted during combustion”, Polymer Degradation and Stability, 113, 2015, 197-207, DOI: 10.1016/j.polymdegradstab.2014.11.015.

DELATOUR V. et FAVRE G., « Le LNE CRM bio 101a est désormais reconnu comme matériau de référence d'ordre supérieur par le JCTLM », Spectra biologie, 217, 2015, 37.

ELORDUI-ZAPATARIETXE S., FETTIG I., PHILIPP R., GANTOIS F., LALERE B., SWART C., PETROV P., GOENAGA-INFANTE H., VANERMEN G., BOOM G. et EMTEBORG H., “Novel concepts for preparation of reference materials as whole water samples for priority substances at nanogram-per-liter level using model suspended particulate matter and humic acids”, Analytical and Bioanalytical Chemistry, 407, 11, 2015, 3055-3067, DOI: 10.1007/s00216-014-8349-8.

ELORDUI-ZAPATARIETXE S., FETTIG I., RICHTER J., PHILIPP R., GANTOIS F., LALERE B., SWART C. et EMTEBORG H., “Interaction of 15 priority substances for water monitoring at ng L21 levels with glass, aluminium and fluorinated polyethylene bottles for the containment of water reference materials”, Accreditation and quality assurance, 20, 6, 2015, 447-455, DOI: 10.1007/s00769-015-1150-3.

GAIE-LEVREL F., MOTZKUS C., MACE T. et VASLIN-REIMANN S., « Développement d’une méthode d’étalonnage pour les instruments de mesure de concentration massique particulaire dans l’air ambiant », Revue française de métrologie, 38, 2015, 11-18, DOI: 10.1051/rfm/2015006.

GEHIN E., BEN-OTHMANE M., HAVET M., SOLLIEC C. et MOTZKUS C., “An experimental approach to measure particle deposition in large circular ventilation ducts”, Environmental Science and Pollution Research international, 22, 7, 2015, 4873-4880.

GONZALEZ-ANTUNA A., RODRIGUEZ-GONZALE Z.P., OHLENDORF R., HENRION A., DELATOUR V. et GARCIA ALONSO J.I., “Determination of Cystatin C in human serum by isotope dilution mass spectrometry using mass overlapping peptides”, Journal of Proteomics, 112, 2015, 141-155, DOI: 10.1016/j.jprot.2014.09.005.

GUILLAUME E. et SARAGOZA L., “Application of FTIR analyzers to fire gases-Progress in apparatus and method validation for quantitative analysis”, Fire and Materials 2015 - 14th International Conference and Exhibition, San Francisco, Etats-Unis d’amérique, 162-174, 2-4 février 2015.

GUILLAUME E., SARAGOZA L., WAKATSUKI K. et BLOMQVIST P., “Effect of gas cell pressure in FTIR analysis of fire effluents”, Fire and Materials, 39, 7, 2015, 675-684, DOI: 10.1002/fam.2273.

HIOKI A., ASAKAI T., MAKSIMOV I., SUZUKI T., MIURA T. et FISICARO P., “Report of the key comparison APMP.QM-K19 - APMP comparison on pH measurement of borate buffer”, Metrologia, 52, Techn. suppl., 2015, 08003, DOI: 10.1088/0026-1394/52/1A/08003.

LABARRAQUE G., OSTER C., FISICARO P., MEYER C., VOGL J., NOORDMANN J., RIENITZ O., RICCOBONO F. et DONET S., “Reference measurement procedures for the quantification of platinum group elements (PGEs) from automotive exhaust emissions”, International journal of environmental analytical chemistry, 95, 9, 2015, 777-789, DOI: 10.1080/03067319.2015.1058931.

MIEGE C., MAZZELLA N., ALLAN I., DULIO V., SMEDES F., TIXIER C., VERMEIRSSEN E., BRANT J., O'TOOLE S., BUDZINSKI H., GHESTEM J-P., STAUB P-F., LARDY-FONTAN S., GONZALEZ J-L., COQUERY M. et VRANA B., “Position paper on passive sampling techniques for the monitoring of contaminants in the aquatic environment - Achievements to date and perspectives”, Trends in Environmental Analytical Chemistry, 8, 2015, 20-26, DOI: 10.1016/j.teac.2015.07.001.

OSTER C., LABARRAQUE G. et FISICARO P., “Certification of a reference material of metal content in atmospheric particles deposited on filters”, Analytical and Bioanalytical Chemistry, 407, 11, 2015, 3035-3043, DOI: 10.1007/s00216-014-8194-9.

OUNOUGHENE G., LE BIHAN O., CHIVAS-JOLY C., MOTZKUS C., LONGUET C., DEBRAY B., JOUBERT A., LE COQ L. et LOPEZ CUESTA J.-M., “Behavior and Fate of Halloysite Nanotubes (HNTs) When Incinerating PA6/HNTs Nanocomposite”, Environmental Science and Technology, 49, 9, 2015, 5450-5457, DOI: 10.1021/es505674j.

PALOS M., DEL CASTILLO, BUSTO M.E., HATTCHOUEL J.-M., PANNIER F., FISICARO P. et VASLIN-REIMANN S., « Développement d’une méthode primaire pour la détermination du fer total dans du sérum », Revue française de métrologie, 40, 2015, 41-50, DOI: 10.1051/rfm/2015015.

YVER KWOK C., LAURENT O., GUEMRI A., PHILIPPON C., WASTINE B. et KAISER C., “Comprehensive laboratory and field testing of cavity ring-down spectroscopy analyzers measuring H2O, CO2, CH4 and CO”, Atmospheric Meas. Techniques, 8, 9, 2015, 3867-3892, DOI: 10.5194/amt-8-3867-2015.

Communications

GUILLAUME E. et SARAGOZA L., “Application of FTIR analyzers to fire gases-Progress in apparatus and method validation for quantitative analysis”, Fire and Materials 2015 - 14th International Conference and Exhibition, San Francisco, Etats-Unis d’amérique, 162-174, 2-4 février 2015.

DEL CASTILLO BUSTO M.E., OSTER C., NUNEZ S., RAAB A., KONOPKA A., LEHMANN W.-D., GOENAGA-INFANTE H. et FISICARO P., “Comparison of different quantification methods for the determination of selenoproteins in human serum: Focus on selenoprotein P”, European Winter Conference on Plasma Spectrochemistry 2015 (EWCPS 2015), Münster, Allemagne, 22-26 février 2015.

FETTIG I., PIECHOTTA C., ALASONATI E., SWART C., KOSCHORRECK J. et FISICARO P., “Traceability for mercury measurements”, European Winter Conference on Plasma Spectrochemistry 2015 (EWCPS 2015), Münster, Allemagne, 22-26 février 2015.

FISICARO P., ALASONATI E., ENT H., SWART C., GOENAGA-INFANTE H. et HORVAT M., “Development of a European metrological infrastructure for mercury measurements”, European Winter Conference on Plasma Spectrochemistry 2015 (EWCPS 2015), Münster, Allemagne, 22-26 février 2015.

KONOPKA A., WINTER D., KONOPKAW., DEL CASTILLO BUSTO M.E., NUNEZ S., GOENAGA-INFANTE H., FISICARO P., BULSKA E. et LEHMANN W.-D., “Novel full-length [Sec-to-Cys]selenoprotein standards for human selenoprotein P and glutathione peroxidase 3 for quantitative proteomics”, European Winter Conference on Plasma Spectrochemistry 2015 (EWCPS 2015), Münster, Allemagne, 22-26 février 2015.

SCHÜTZE M., WERIAN A., SWART C., RIENITZ O., BIESTER H., FISICARO P. et GOENAGA-INFANTE H., “Traceability for speciation of mercury in water and isotopic ratio measurements”, European Winter Conference on Plasma Spectrochemistry 2015 (EWCPS 2015), Münster, Allemagne, 22-26 février 2015.

SWART C., TOKMAN N., RAAB A., JAKUBOWKS, N., DEL CASTILLO M.-E., GOENAGA-INFANTE H., KONOPKA A., ZAKEL S. et BERNEVIC B, “Development of reference measurement procedures for metalloproteins (EMRP HLT 05 Metallomics)”, European Winter Conference on Plasma Spectrochemistry 2015 (EWCPS 2015), Münster, Allemagne, 22-26 février 2015.

DELATOUR V., « Evaluation de la justesse des méthodes de dosage de biomarqueurs en biochimie clinique : importance de la commutabilité et des méthodes de référence », Séminaire « Métrologie en biologie médicale », Hôpital Européen Georges Pompidou, Paris, France, 6 mars 2015.

CLOUET FORAISON N., GAIE-LEVREL F. et DELATOUR V., « Application de l’analyse par mobilité différentielle à la caractérisation de bio-nanoparticules », 1er congrès francophone de l’AFSEP, Paris, France, 31 mars - 2 avril 2015.

MACÉ T., GAIE-LEVREL F. et MOTZKUS C., “Overview of LNE's activities led in aerosol metrology”, Particulate Workshop (BIPM), Sèvres, France, 15 avril 2015.

BROS P., DELABY C., DELATOUR V., MOULINIER A., CAZALS G., VIALARET J., LEHMANN S. et HIRTZ C., “Towards a reference method for absolute quantification of hepcidin-25 in serum by mass spectrometry”, Congrès Euromedlab/IFCC, Paris, France, 21-25 juin 2015.

CLOUET-FORAISON N., GAIE-LEVREL F., KAMMEL M., DIVIETO C., PARKS H. et DELATOUR V., Standardization in advanced Lipoprotein testing: The BioSITrace project, Congrès Euromedlab/IFCC, Paris, France, 21-25 juin 2015.

FISICARO P., ENT H., SWART C., DUNN P. et HORVAT M., “Development of a metrological infrastructure for mercury measurements”, ICMGP 2015 Korea, Jeju, Corée, 22-26 juin 2015.

DEL CASTILLO BUSTO M.E., OSTER C., NUNEZ S., RAAB A., KONOPKA A., LEHMANN W.D., GOENAGA-INFANTE H. et FISICARO P., “Isotope dilution mass spectrometry as a traceable tool to assess selenium status in humans”, Euromedlab Satellite meeting “State of the art in the biology of trace elements and vitamins”, Paris, France, 26-27 juin 2015.

PALOS M., DEL CASTILLO BUSTO M.E., PANNIER F., SWART C., BRAUCKMANN C. et FISICARO P., “Reference methods for iron and haemoglobin by isotope dilution inductively coupled plasma mass spectrometry (ID-ICP-MS) to assess metrological traceability in clinical biochemistry”, Euromedlab Satellite meeting “State of the art in the biology of trace elements and vitamins”, Paris, France, 26-27 juin 2015.

BRIEUDES V., LARDY-FONTAN S., LALERE B., VASLIN-REIMANN S. et BUDZINSKI H., “Method validation and uncertainties evaluation for more reliable measurements of drug residues in the environment: a case study on the Seine river”, Workshop: Mediterranean Sea Region Countries Mass Spectrometry Workshop (MEDMS III), Athènes, Grèce, 28 juin - 2 juillet 2015.

MACÉ T., “The national laboratory for air quality monitoring (LCSQA): a 25 years feedback, The third International Conference on Environmental Specimen Banks, Nancy, France, 30 juin - 1er juillet 2015.

PALOS M., DEL CASTILLO BUSTO M.E., BRAUCKMANN C., SWART C., POTIN-GAUTIER M., PANNIER F. et FISICARO P., “Reference methods for total haemoglobin by isotope dilution inductively coupled plasma mass spectrometry to assess metrological traceability in clinical biochemistry”, Euroanalysis 2015, Bordeaux, France, 6-10 septembre 2015.

DESENFANT M., ALLARD A., LALERE B., LARDY-FONTAN S., LE DIOURON V., LEPOT B. et ZIEGLER E., « Comparaison de différentes stratégies d'évaluation de la performance dans les essais d'aptitude par comparaison interlaboratoire », 17e Congrès international de métrologie, Paris, France, 21-24 sept. 2015.

FISICARO P., ENT H., SWART C., DUNN P. et HORVAT M., “Traceability for mercury measurements”, 17e Congrès international de métrologie, Paris, France, 21-24 septembre 2015 DOI: 10.1051/metrology/20150007001.

GAIE-LEVREL F. , MOTZKUS C. et MACÉ T., “Development of a calibration method for on-line analyzer of atmospheric particle mass concentrations, 17e Congrès international de métrologie, Paris, France, 21-24 septembre 2015, DOI: 10.1051/metrology/20150007002.

GAIE-LEVREL F., MOTZKUS C. et MACÉ T., “Metrological characterisation of the size distribution of airborne nanoparticles generated from nanomaterials in the form of colloidal suspension, 17e Congrès international de métrologie, Paris, France, 21-24 septembre 2015.

LARDY-FONTAN S., Development and implementation of a DI-MS based method with full uncertainty estimate to achieve measurement of pharmaceutical residus in natural waters, 17e Congrès international de métrologie, Paris, France, 21-24 septembre 2015, DOI: 10.1051/metrology/20150005001.

LARDY-FONTAN S., CHATELLIER C., LESTREMAU F., LALERE B. et STRUB M-P., Reliability of organic compounds measurement in enviromental monitoring. The key role of analytical standard substance. A study case on alkylphenols”, 17e Congrès international de métrologie, Paris, France, 21-24 septembre 2015, DOI: 10.1051/metrology/20150007010.

PALOS M., DEL CASTILLO BUSTO M.E., PANNIER F., SWART C., BRAUCKMANN C. et FISICARO P., « Détermination de l’hémoglobine totale par dilution isotopique ICP-MS afin d’assurer la traçabilité métrologique en biochimie clinique », 17e Congrès international de métrologie, Paris, France, 21-24 septembre 2015, DOI: 10.1051/metrology/20150009005.

LARDY-FONTAN S. et al., “Metrology applied to the survey of pharmaceutical residues in water for a better protection of consumers”, Workshop: “Food metrology: Approaches and tools for measuring food quality”, Milan, Italie, 9 octobre 2015.

SWART C., GLEITZMANN J., TOKMAN N., RAAB A., DEL CASTILLO BUSTO M.E., BRAUCKMANN C., ZAKEL S., ARSENE C.-G., FRANK C. et NEUKAMMER J., “Candidate reference measurement procedures for metalloproteins for the characterisation of future reference materials”, 14th International Symposium on Biological and Environmental Reference Materials (BERM 14), Maryland, États-Unis, 11-15 octobre 2015.

FISICARO P., “How to increase impact of research activities in metrology: the example of some joint research projects in the field of chemistry”, 16th Beijing Conference and Exhibition on Instrumental Analysis (BCEIA), Beijing, Chine, 27-30 oct. 2015.

CLOUET FORAISON N., GAIE-LEVREL F. et DELATOUR V., “Establishing metrological traceability in advanced Lipoprotein testing:  The Bio-SITrace project”, APMP meeting 2015 – TCQM Workshop, Beijing, Chine, 29 octobre - 7 novembre 2015.

DELATOUR V., “A commutability study coupled with a multi-centric analysis of accuracy of glucose, creatinine, total cholesterol, total glycerides, LDL-C and HDL-C assays”, 14th International Symposium on Biological and Environmental Refe-rence Materials, Washington, États-Unis, 11-15 octobre 2015.

SWART C., GLEITZMANN J., TOKMAN N., RAAB A., DEL CASTILLO E., BRAUCKMANN C., ZAKEL S., ARSENE C.-G. et FRANK C., “New approach for the development of candidate reference measurement procedures”, JCTLM 2015: Meeting of JCTLM Members and Stakeholders, Sèvres, France, 30 novembre – 1er décembre 2015.

LARDY-FONTAN S., LALERE B. et VASLIN-REIMANN S., “Metro-logy to support a validated effect based monitoring strategy within the Water Framework Directive (WFD-2013/60/EC). Proof of concept for high concern pollutants”, Workshop: Presentation of ideas in preparation for the targeted programme “Environment” in 2016, Turin, Italie, 1er décembre 2015.

DELABY S., GAIE-LEVREL F., WIART M. et BENCSIK A., “Impact on the nervous system of particles released from nanocomposite materials under stress use (Release_NanoTox)”, European Nanomedicine Meeting (ENM 2015), Grenoble, France, 7-9 décembre 2015.

Abstract

Day after day, new applications using manufactured nanoparticles appear in industry. To evaluate the occupational risk associated to nanoparticles, it is important to have reliable, accurate and standardized measurement methods. It is therefore necessary to work on pre-normalization projects to develop reference methods to characterize the number and the size distribution of airborne nanoparticles. The aim of this pre-normalization project is to develop characterization methods for airborne nanoparticles that include all the measurement chain (sampling, analysis, data treatments, etc.) which will be traceable, adequate and accurate: this project includes the estimation of the uncertainties on the measurements. This presented study, first step of this project, describes the generation and the characterization of SiO2 airborne nanoparticles from a liquid manufactured suspension. Experiments have been performed in order to study the stability and the repeatability of the generation protocol of SiO2 airborne nanoparticles by measuring their count size distributions with a Scanning Mobility Particle Sizer (SMPS).

Key words

aérosol
nanoparticle
microscopy
scanning mobility particle sizer
atomization

Abstract

pH measurements of seawater are suffering of a lack of spatiotemporal compatibility and comparability. The present paper makes an analysis of the current state of art of seawater pH measurement. The theoretical problemes, such as the definition of the activity coefficient, and practical problemes related especially to the complex matrix are pointed out. The necessary actions to overcome theses difficulties are also described. They are part of an European Joint Research Project entituled “Metrology for the salinity and ocean acidification” and funded by EMRP. Some preliminary results obtained for a saline solution containing only NaCl are presented in order to show the influence of the matrix on the experimentally obtained acidity functions.

Key words

pH
ARTIFICIAL SEAWATER TRACEABILITY
POTENTIOMETRY
SPECTROPHOTOMETRY
TRIS

Abstract

This work presents the development of a reference method by ICP-MS for the determination of iron in serum. To ensure the metrological traceability of the results, isotope dilution associated with ICP-MS (ID-ICP-MS) has been applied, which has the potential to be a primary measurement procedure. Method validation has been demonstrated through the use of a certified reference material (SRM 1598a) and the participation in an international comparison between National Metrology Institutes (BIPM-CCQM K107). The validated method is now available to support clinical laboratories in the evaluation of their measurement capabilities and for quality assurance and quality control programmes. In fact, this ID-ICP-MS method can be used to certify reference materials or to assign reference values to samples used in proficiency testing schemes. The feasibility has been tested on two unknown samples, i.e. BCR® -637, IRMM sample and an ANSM B17 sample (a material distributed during a National Quality Control programme).

Key words

metrological traceability
isotope dilution
iron
sérum
icp-ms
primary measurement procedure
biomedical analysis

Abstract

To ensure the water quality in Europe, the European Commission asked the member states to provide comparable and traceable measurement results for the analysis of critical pollutants. Considering the increasing environmental challenges, the contribution of metrology is necessary both for the improvement of analysis reliability and the comparability of results. For this reason the European research project Euramet/EMRP/ENV08 “Traceable measurements for monitoring critical pollutants under the European Water Framework Directive (WFD-2000/60/EC)”, funded by the EMRP, aimed to provide the elements for the development of a metrological basis. The project develops primary reference methods enabling the analysis of priority hazardous substances in order to meet the WFD requirements in terms of performance levels (limit of quantification and uncertainties). Polycyclic aromatic hydrocarbons (PAHs) – priority hazardous substances for which no DCE compatible methods exist – are among the three families of pollutants targeted by the project. This paper tackles the development and validation of the PAH analysis method on whole water samples. The method that best meets the requirements of the WFD in terms of level of concentration and uncertainty is the solid phase extraction (SPE) method with SPE-disks, followed by isotope dilution analysis combined with gas chromatography mass spectrometry (ID-GC/MS).

Key words

PAH
reference methods
limit of quantification
uncertainty
spe disk

Abstract

The TEOM-FDMS (Tapered Element Oscillating Microbalance with Filter Dynamics Measurement Systems) is a common measuring instrument employed by the French air quality monitoring network.This instrument is currently calibrated with calibration weights traceable to SI but having values and masses differences between each of them which are not representative of real atmospheric particle mass measurements. Moreover, these calibration weights do not allow detecting any technical problem of the TEOM-FDMS sampling system upstream the mass measurement and of the intrinsic TEOM-FDMS filtration system. In this way, a calibration method was developed using a portable particle generator system producing known and stable particle mass concentrations over time. In this paper, we present the characterization of this portable generation system in terms of reference range of particle masses, its coupling with four different TEOM-FDMS and the global comparison between the defined reference range of particle masses and the averaged weighed and measured masses obtained with each TEOM-FDMS implicated in this study.

Key words

generator
particle
aérosol
mass concentration
particulate mass
calibration
teom-fdms